Technology Process of C30H35FN4O2
There total 12 articles about C30H35FN4O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium azide / N,N-dimethyl-formamide
2: 5%-palladium/activated carbon; hydrogen
3: ammonia / methanol
4: sodium tris(acetoxy)borohydride / dichloromethane
5: hydrogenchloride / methanol
6: triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate
With
hydrogenchloride; sodium azide; 5%-palladium/activated carbon; ammonia; hydrogen; sodium tris(acetoxy)borohydride; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.113
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydroxide / methanol / Heating
2: palladium 10% on activated carbon; hydrogen
3: hydrogenchloride / water; acetonitrile
4: sodium tris(acetoxy)borohydride / dichloromethane
5: hydrogenchloride / methanol
6: triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; potassium hydroxide;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.09.113
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydroxide / methanol / Heating
2: palladium 10% on activated carbon; hydrogen
3: hydrogenchloride / water; acetonitrile
4: sodium tris(acetoxy)borohydride / dichloromethane
5: hydrogenchloride / methanol
6: triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; potassium hydroxide;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.09.113