1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol

Base Information

Chemical Name:1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol
CAS No.:672959-00-1
Molecular Formula:C₃₈H₃₀Fe₂O₂
Molecular Weight:630.349
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol

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Technology Process of 1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol

There total 1 articles about 1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.6%

: 1272-44-2
benzoylferrocene

: 4526-07-2
1,4-bis(trimethylsilyl)-1,3-butadiyne

: 32983-19-0
1-ferrocenyl-1-phenylpenta-2,4-diynol

: 672959-00-1
1,6-diferrocenyl-1,6-diphenylhexa-2,4-diyn-1,6-diol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; n-BuLi in pentane was added at -60° C under Ar to a THF soln. of silylated butadiyne, warmed to room temp., FcCOPh was added under Ar, the mixt. was stirred for 60 h at room temp.; water was added, volatiles removed in vacuo, residue was dissolved in CH2Cl2, soln. washed with water, dried over Na2SO4, evapd., residue was chromd. on basic alumina (eluent 1:1 hexane-ether); elem. anals.;