1,6-diferrocenyl-1,6-diphenylhexapentaene

Base Information

Chemical Name:1,6-diferrocenyl-1,6-diphenylhexapentaene
CAS No.:673460-88-3
Molecular Formula:C₃₈H₂₈Fe₂
Molecular Weight:596.334
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-diferrocenyl-1,6-diphenylhexapentaene

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Technology Process of 1,6-diferrocenyl-1,6-diphenylhexapentaene

There total 2 articles about 1,6-diferrocenyl-1,6-diphenylhexapentaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.6%

: 672958-80-4
1-ferrocenyl-1-methoxy-1-phenylpropyne

: 673460-88-3,672958-97-3
1,6-diferrocenyl-1,6-diphenylhexapentaene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; byproducts: MeOLi, 1-ferrocenyl-1-phenylpropynol; n-BuLi in pentane was added at -60°C under Ar to a THF soln. of FcPh(HO)CCCH, soln. was warmed to room temp. to give the red colour of Li-deriv., the mixt. was refluxed under Ar for 12 h; filtd. through a short column of basic alumina, filtrate evapd., residuechromd. as quickly as possible on a basic alumina column (eluent 1:5 he xane-ether), eluate evapd.; TLC data, elem. anal.;