(η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate

Base Information

Chemical Name:(η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate
CAS No.:72804-54-7
Molecular Formula:C₁₁H₁₁Ru*C₂₄H₂₀B
Molecular Weight:563.512
Hs Code.:

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Chemical Property of (η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate

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Technology Process of (η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate

There total 1 articles about (η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: cyclopentadienylthallium(I)

: 143-66-8
sodium tetraphenyl borate

: 72804-54-7
(η(6)-benzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium tetraphenylborate

Guidance literature:: In water; acetonitrile; N2-atmosphere; stirring Ru-complex with excess TlCp (in dark, in MeCN, 5h), filtration, addn. of H2O, filtration, addn. of excess NaBPh4 (in H2 O), stirring for 30 min; pptn. on concn., filtration, washing (H2O), drying (vac.); can be recrystallized (MeCN/Et2O); elem. anal.;
DOI:10.1016/0022-328X(95)05717-4