3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

Base Information

Chemical Name:3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester
CAS No.:87363-56-2
Molecular Formula:C₃₁H₄₂N₄O₁₆
Molecular Weight:726.692
Hs Code.:

3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

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Chemical Property of 3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

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Technology Process of 3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

There total 2 articles about 3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: Acetic acid (2R,3R,4S,5S,6R)-3,5-diacetoxy-2-acetoxymethyl-6-(6-amino-hexanoylamino)-tetrahydro-pyran-4-yl ester

: 87363-66-4
tert-butyl 2-chloro-3,5-dinitrobenzoate

: 87363-56-2
3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

Guidance literature:: With 4-methyl-morpholine; In 1,4-dioxane; for 24h; Ambient temperature;
DOI:10.1002/hlca.19830660413

Reference yield:

: 2497-91-8
2-chloro-3,5-dinitrobenzoic acid

: 87363-56-2
3,5-Dinitro-2-[5-((2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylcarbamoyl)-pentylamino]-benzoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / 70percent HClO₄ / 5 h / Ambient temperature

2: 24 percent / 4-methylmorpholine / dioxane / 24 h / Ambient temperature

With 4-methyl-morpholine; perchloric acid; In 1,4-dioxane;
DOI:10.1002/hlca.19830660413