(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)]BF₄

Base Information

• Chemical Name: (C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)]BF₄
• CAS No.: 190839-80-6
• Molecular Formula: BF₄*C₃₀H₃₃MoN₂O₂P₂
• Molecular Weight: 698.296
• Mol file: 190839-80-6.mol

Synonyms:

Chemical Property of (C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)]BF₄

There total 1 articles about (C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Mo(P(C₆H₅)3)(CO)2(N(CH₃)CH₂CH₂N(CH₃)PCH₃)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(C5H5)Mo(CH3)(CO)2(N(CH3)CH2CH2N(CH3)POCH3) (190839-66-8) + trifluoroborane diethyl ether (109-63-7) + triphenylphosphine (603-35-0) → (C5H5)Mo(P(C6H5)3)(CO)2(N(CH3)CH2CH2N(CH3)PCH3)(1+)*BF4(1-)=[(C5H5)Mo(P(C6H5)3)(CO)2(N(CH3)CH2CH2N(CH3)PCH3)]BF4 (190839-80-6)

Guidance literature:

In dichloromethane; N2-atmosphere; addn. of 2 equiv. of B-compd. to Mo-complex soln. at -78°C, warming to room temp., stirring for 1 h, cooling to -78°C, addn. of 1.2 equiv. PPh3, warming to room temp., stirring for 12 h; concn. (vac.), chromy. (in air, Al2O3, CH2Cl2, then CH2Cl2/Me2CO=10:1), solvent removal (vac.); elem. anal.;

DOI:10.1016/S0022-328X(96)06615-6

upstream raw materials:

(C₅H₅)Mo(CH₃)(CO)2(N(CH₃)CH₂CH₂N(CH₃)POCH₃)

trifluoroborane diethyl ether

triphenylphosphine