Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)

Base Information

Chemical Name:Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)
CAS No.:79132-42-6
Molecular Formula:C₃₄H₂₀Mo₂O₁₀Sb₂
Molecular Weight:1023.91
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)

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Technology Process of Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)

There total 2 articles about Tetraphenyl-distiban-bis(pentacarbonylmolybdaen) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 2654-44-6
tetraphenyldistibane

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 79132-42-6
Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); under Ar Mo(CO)6 in THF was irradiated for 5 h, then the Sb-ligand in THF added and left at 4°C overnight; the solvent evapd. in vac., the residue washed with pentane, pptd. at -25°C, excess Mo(CO)6 evapd. in vac., the residue crystd. from pentane; elem. anal.;

Reference yield: 29.0%

: 2654-44-6
tetraphenyldistibane

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 79132-42-6
Tetraphenyl-distiban-bis(pentacarbonylmolybdaen)

: 79132-47-1
Bis-μ-diphenylantimonido-bis(tetracarbonylmolybdaen)

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); Mo(CO)6 in THF was irradiated for 5 h under Ar, then the Sb-ligand was added; THF was distd. off, the residue washed with pentane, pptd. at -25°C, bispentacarbonyl product sublimated, the residue washed with pentane; elem. anal.;