-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Base Information

Chemical Name:-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate
CAS No.:130584-57-5
Molecular Formula:C₂₅H₄₂O₅Si
Molecular Weight:450.691
Hs Code.:

<R-(E,Z)>-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Synonyms:

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Chemical Property of -methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Chemical Property:

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Technology Process of -methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

There total 8 articles about -methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130584-48-4
(R)-1-phenoxy-3-(prop-2-enyloxy)propan-2-ol

: 130584-57-5,130584-58-6
-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / imidazole / dimethylformamide / 18 h

2: 1) O₃, Sudan III, 2) Ph₃P / 1) CH₂Cl₂, -78 deg C, 1.5 h, 2) -78 deg C to 20 deg C, 1 h

3: 1) KO-t-Bu / 1) THF, 20 deg C, 1 h, 2) THF, 4 h

4: diethyl ether

5: 1) H₂, (C₈H₁₂)IrH₂(PPh₂Me)2 / 1) THF, 3 min, 2) 2 days

With 1H-imidazole; oil scarlet; (C₈H₁₂)IrH₂(PPh₂Me)2; potassium tert-butylate; hydrogen; ozone; triphenylphosphine; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 130584-49-5
(R)-t-butyldimethyl<1-(phenoxymethyl)-2-(prop-2-enyloxy)ethoxy>silane

: 130584-57-5,130584-58-6
-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) O₃, Sudan III, 2) Ph₃P / 1) CH₂Cl₂, -78 deg C, 1.5 h, 2) -78 deg C to 20 deg C, 1 h

2: 1) KO-t-Bu / 1) THF, 20 deg C, 1 h, 2) THF, 4 h

3: diethyl ether

4: 1) H₂, (C₈H₁₂)IrH₂(PPh₂Me)2 / 1) THF, 3 min, 2) 2 days

With oil scarlet; (C₈H₁₂)IrH₂(PPh₂Me)2; potassium tert-butylate; hydrogen; ozone; triphenylphosphine; In diethyl ether;

Reference yield:

: 130584-55-3
(R)-2-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-ethanal

: 130584-57-5,130584-58-6
-methyl 9-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>non-8-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) KO-t-Bu / 1) THF, 20 deg C, 1 h, 2) THF, 4 h

2: diethyl ether

3: 1) H₂, (C₈H₁₂)IrH₂(PPh₂Me)2 / 1) THF, 3 min, 2) 2 days

With (C₈H₁₂)IrH₂(PPh₂Me)2; potassium tert-butylate; hydrogen; In diethyl ether;