Technology Process of C24H34N2O8
There total 1 articles about C24H34N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-cyanobenzoic acid methyl ester;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
di-tert-butyl dicarbonate;
With
dmap;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium hydroxide
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol
3.1: tetrabutyl ammonium fluoride
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 h / 0 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
5.2: Saturated solution
With
tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hydroxide;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium hydroxide
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol
3: tetrabutyl ammonium fluoride
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
N,N-dimethyl-formamide;