C₁₉H₁₇BrO₇S

Base Information

Chemical Name:C₁₉H₁₇BrO₇S
CAS No.:891148-72-4
Molecular Formula:C₁₉H₁₇BrO₇S
Molecular Weight:469.31
Hs Code.:

C<sub>19</sub>H<sub>17</sub>BrO<sub>7</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₇BrO₇S

Chemical Property:

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Technology Process of C₁₉H₁₇BrO₇S

There total 4 articles about C₁₉H₁₇BrO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-68-5
methyl-phenyl-thioether

: 891148-72-4
C₁₉H₁₇BrO₇S

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / chloroform / 2 h / 20 °C

2.1: phosphoric acid; dihydrogen peroxide / acetic acid / 3 h / Reflux

3.1: morpholine; sulfur / 10 h / 130 °C

3.2: 10 h / 85 °C

4.1: acetic anhydride; triethylamine / 3 h / 130 - 140 °C

With morpholine; aluminum (III) chloride; phosphoric acid; dihydrogen peroxide; acetic anhydride; sulfur; triethylamine; In chloroform; acetic acid; 1.1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2010.12.063

Reference yield:

: 1778-09-2
4-(Methylthio)acetophenone

: 891148-72-4
C₁₉H₁₇BrO₇S

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoric acid; dihydrogen peroxide / acetic acid / 3 h / Reflux

2.1: morpholine; sulfur / 10 h / 130 °C

2.2: 10 h / 85 °C

3.1: acetic anhydride; triethylamine / 3 h / 130 - 140 °C

With morpholine; phosphoric acid; dihydrogen peroxide; acetic anhydride; sulfur; triethylamine; In acetic acid;
DOI:10.1016/j.bmcl.2010.12.063

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 891148-72-4
C₁₉H₁₇BrO₇S

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / methanol / 3 h / 20 °C

2: acetic anhydride; triethylamine / 3 h / 130 - 140 °C

With bromine; acetic anhydride; triethylamine; In methanol;
DOI:10.1016/j.bmcl.2010.12.063