[Ir(C₆H₄SNCC₁₂H₈)2Cl]2

Base Information

Chemical Name:[Ir(C₆H₄SNCC₁₂H₈)2Cl]2
CAS No.:865377-25-9
Molecular Formula:C₇₆H₄₈Cl₂Ir₂N₄S₄
Molecular Weight:1600.85
Hs Code.:

[Ir(C<sub>6</sub>H<sub>4</sub>SNCC<sub>12</sub>H<sub>8</sub>)2Cl]2

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Chemical Property of [Ir(C₆H₄SNCC₁₂H₈)2Cl]2

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Technology Process of [Ir(C₆H₄SNCC₁₂H₈)2Cl]2

There total 1 articles about [Ir(C₆H₄SNCC₁₂H₈)2Cl]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67362-98-5
2-([1,1′-biphenyl]-4-yl)benzo[d]thiazole

: iridium(III) chloride hydrate

: 865377-25-9
[Ir(C₆H₄SNCC₁₂H₈)2Cl]2

Guidance literature:: In 2-ethoxy-ethanol; water; under Ar; by refluxing IrCl3*nH2O (1 mmol) with a ligand (2.4 mmol) in amixt. of 2-ethoxyethanol and H2O (3:1) at 110°C; according to F. O. Garces et al. Inorg. Chem., 1988, 27, 3464; S. Spouse et al. J. Am. Chem. Soc., 1984, 106, 6647; the ppt. was filtered and washed with aq. soln. of HCl and methanol, then dried under vac.;
DOI:10.1039/c1dt10305a

Reference yield: 45.0%

: 865377-25-9
[Ir(C₆H₄SNCC₁₂H₈)2Cl]2

: 123-54-6,81235-32-7
acetylacetone

: 1315610-19-5
bis[2-(biphenyl-4-yl)benzothiazole-N,C²']iridium(III)(acetylacetonate)

Guidance literature:: With sodium carbonate; In 2-ethoxy-ethanol; under Ar; by refluxing Ir-contg. compd. (0.1 mmol), acetylacetone (0.3 mmol) and Na2CO3 (1 mmol) in 2-ethoxyethanol for 12 h (110°C); after cooling, the ppt. was collected; flash chromy. (silica, CHCl3 as eluent); 3 recrystns.; the compd. was dried for 24 h at 100°C under vac. (1.5 kPa); elem. anal.;
DOI:10.1039/c1dt10305a