methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

Base Information

Chemical Name:methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde
CAS No.:79693-56-4
Molecular Formula:C₁₁H₁₈O₂
Molecular Weight:182.263
Hs Code.:

Synonyms:

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Chemical Property of methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

Chemical Property:

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Technology Process of methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

There total 8 articles about methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 79693-55-3
methylene-2 methoxy-5 dimethyl-6,6 cyclohexyle-2 dithianne-1,3

: 79693-56-4
methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

Guidance literature:: With mercury dichloride; mercury(II) oxide; In acetonitrile; Heating;

Reference yield:

: 4454-05-1
2-methoxy-3,4-dihydro-2H-pyran

: 79693-56-4
methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

Guidance literature:: Multi-step reaction with 8 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 84 percent / carbon tetrabromide, triphenylphosphine / acetonitrile / 3 h / Heating

6: 80 percent / 48 h / Ambient temperature

7: 84 percent / 1.5 M butyllithium / tetrahydrofuran; hexane

8: 60 percent / mercury(II) chloride, mercury(II) oxide / acetonitrile / Heating

With sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex; triphenylphosphine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; hexane; water; acetic acid; acetonitrile;

Reference yield:

: 4454-02-8
1,1,5,5-tetramethoxy-pentane

: 79693-56-4
methylene-2 trans-methoxy-5 dimethyl-6,6 cyclohexane formaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 61 percent / boron trifluoride etherate / Ambient temperature

2: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

3: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

4: 84 percent / carbon tetrabromide, triphenylphosphine / acetonitrile / 3 h / Heating

5: 80 percent / 48 h / Ambient temperature

6: 84 percent / 1.5 M butyllithium / tetrahydrofuran; hexane

7: 60 percent / mercury(II) chloride, mercury(II) oxide / acetonitrile / Heating

With sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; boron trifluoride diethyl etherate; sodium acetate; triphenylphosphine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; hexane; water; acetic acid; acetonitrile;