3,6-dimethyl-4-phenylcyclohexene

Base Information

• Chemical Name: 3,6-dimethyl-4-phenylcyclohexene
• CAS No.: 1384840-63-4
• Molecular Formula: C₁₄H₁₈
• Molecular Weight: 186.297
• Mol file: 1384840-63-4.mol

Synonyms:

Chemical Property of 3,6-dimethyl-4-phenylcyclohexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-dimethyl-4-phenylcyclohexene

There total 1 articles about 3,6-dimethyl-4-phenylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + hexa-2,4-diene (592-46-1) → 3,6-dimethyl-4-phenylcyclohexene (1384840-63-4,19003-62-4,19003-63-5)

Guidance literature:

With hydroquinone; at 60 ℃; for 30h; Inert atmosphere;

DOI:10.1007/s11172-011-0322-5

Reference yield: 64.0%

3,6-dimethyl-4-phenylcyclohexene (1384840-63-4,19003-62-4,19003-63-5) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6) → η6-[(3,6-dimethylcyclohexen-4-yl)benzene]chromium tricarbonyl (1384525-90-9)

Guidance literature:

In octane; diethylene glycol dimethyl ether; ligand, Cr(CO)6 and diglyme-octane 1:1 refluxed at 160°C for 18 hunder Ar; filtered with Al2O3 layer, solvent evapd. in vacuo;

DOI:10.1007/s11172-011-0322-5

upstream raw materials:

styrene

hexa-2,4-diene

Downstream raw materials:

η6-[(3,6-dimethylcyclohexen-4-yl)benzene]chromium tricarbonyl