C₂₀H₂₉F₂N₃O

Base Information

Chemical Name:C₂₀H₂₉F₂N₃O
CAS No.:1292322-00-9
Molecular Formula:C₂₀H₂₉F₂N₃O
Molecular Weight:365.467
Hs Code.:

C<sub>20</sub>H<sub>29</sub>F<sub>2</sub>N<sub>3</sub>O

Synonyms:

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Chemical Property of C₂₀H₂₉F₂N₃O

Chemical Property:

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Technology Process of C₂₀H₂₉F₂N₃O

There total 14 articles about C₂₀H₂₉F₂N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₇F₂N₃O₃

: 1292322-00-9
C₂₀H₂₉F₂N₃O

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1292322-00-9
C₂₀H₂₉F₂N₃O

Guidance literature:: Multi-step reaction with 14 steps

1: sodium hydride / tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol

3: water; potassium hydroxide / ethanol / 20 °C

4: triethylamine / diethyl ether / 20 °C

5: n-butyllithium / tetrahydrofuran / -78 °C

6: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

7: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

8: hydrogenchloride / tetrahydrofuran; water / 20 °C

9: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 110 °C

10: chloro-trimethyl-silane / dichloromethane / 20 °C

11: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

12: water; sodium hydroxide / ethanol / 20 °C

13: ammonia; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

14: trifluoroacetic acid / dichloromethane / 20 °C

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; ammonia; water; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; sodium tris(acetoxy)borohydride; sodium hydride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 9: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-37-9
C₁₇H₂₀F₂O₄

: 1292322-00-9
C₂₀H₂₉F₂N₃O

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / tetrahydrofuran; water / 20 °C

2: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 110 °C

3: chloro-trimethyl-silane / dichloromethane / 20 °C

4: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

5: water; sodium hydroxide / ethanol / 20 °C

6: ammonia; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

7: trifluoroacetic acid / dichloromethane / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; ammonia; water; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 2: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060