cis-[PtCl₂(HN=C(Ph)ONC(Me)NH₂)2]

Base Information

• Chemical Name: cis-[PtCl₂(HN=C(Ph)ONC(Me)NH₂)2]
• CAS No.: 1374586-38-5
• Molecular Formula: C₁₈H₂₂Cl₂N₆O₂Pt
• Molecular Weight: 620.398
• Mol file: 1374586-38-5.mol

Synonyms:

Chemical Property of cis-[PtCl₂(HN=C(Ph)ONC(Me)NH₂)2]

Chemical Property:

Purity/Quality:

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Technology Process of cis-[PtCl₂(HN=C(Ph)ONC(Me)NH₂)2]

There total 1 articles about cis-[PtCl₂(HN=C(Ph)ONC(Me)NH₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

cis-bis(benzonitrile)dichloroplatinum(II) (14873-63-3) + acetamide oxime (118493-85-9,117771-39-8,1141922-26-0,1429624-21-4) → cis-[PtCl2(HN=C(Ph)ONC(Me)NH2)2] (1374586-38-5,1374649-48-5)

Guidance literature:

In nitromethane; a mixt. of amidoxime and Pt-complex was dissolved in CH3NO2, stirred, kept for 24 h at room temp.; cooled to 4°C, ppt. was filtered off, washed with CHCl3 (2x), dried at room temp. in air; elem. anal.;

DOI:10.1021/ic3006019

Reference yield: 100.0%

cis-[PtCl2(HN=C(Ph)ONC(Me)NH2)2] (1374586-38-5,1374649-48-5) + water (7732-18-5) + silver nitrate → cis-[Pt(NH=C(Me)ONC(Ph)NH2)2](NO3)2*2H2O

Guidance literature:

In methanol; byproducts: AgCl; a mixt. of complex and AgNO3 was suspd. in methanol, kept in the dark for 30 min under vigorous stirring; warm CH3OH was added, AgCl was filtered, evapd. in vac., the residue waswashed with CH2Cl2 and diethyl ether; elem. anal.;

DOI:10.1021/ic3006019

upstream raw materials:

cis-bis(benzonitrile)dichloroplatinum(II)

acetamide oxime