[¹⁴C]SSR₁₄₉₇₄₄

Base Information

Chemical Name:[¹⁴C]SSR₁₄₉₇₄₄
CAS No.:1447931-43-2
Molecular Formula:C₃₄H₄₇NO₄
Molecular Weight:535.74
Hs Code.:

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Chemical Property of [¹⁴C]SSR₁₄₉₇₄₄

Chemical Property:

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Technology Process of [¹⁴C]SSR₁₄₉₇₄₄

There total 9 articles about [¹⁴C]SSR₁₄₉₇₄₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1447931-33-0
C₂₅⁽¹⁴⁾CH₂₉ClO₄

: 111-92-2
dibutylamine

: 1447931-43-2
[¹⁴C]SSR₁₄₉₇₄₄

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile;
DOI:10.1002/jlcr.3009

Reference yield:

: 90919-20-3
4-(3-chloropropyl)benzoic acid

: 1447931-43-2
[¹⁴C]SSR₁₄₉₇₄₄

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / 100 °C

2: iron(III) chloride / 1,2-dichloro-ethane

3: potassium iodide; potassium carbonate / acetonitrile

With iron(III) chloride; thionyl chloride; potassium carbonate; potassium iodide; In 1,2-dichloro-ethane; acetonitrile; 2: |Friedel-Crafts Acylation;
DOI:10.1002/jlcr.3009

Reference yield:

: 937385-02-9
4-(3-chloropropyl)benzoyl chloride

: 1447931-43-2
[¹⁴C]SSR₁₄₉₇₄₄

Guidance literature:: Multi-step reaction with 3 steps

1: iron(III) chloride / 1,2-dichloro-ethane / 4.25 h / 20 °C / Cooling with ice

2: sodium iodide / acetonitrile / 1 h / Microwave irradiation

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-ethyl-N,N-diisopropylamine / 18 h / 70 °C / Cooling with liquid nitrogen

With iron(III) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,2-dichloro-ethane; acetonitrile; 1: |Friedel-Crafts Acylation;
DOI:10.1002/jlcr.3009