C₃₂H₃₅Cl₂N₅O₄

Base Information

Chemical Name:C₃₂H₃₅Cl₂N₅O₄
CAS No.:1197342-23-6
Molecular Formula:C₃₂H₃₅Cl₂N₅O₄
Molecular Weight:624.567
Hs Code.:

C<sub>32</sub>H<sub>35</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₂H₃₅Cl₂N₅O₄

Chemical Property:

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Technology Process of C₃₂H₃₅Cl₂N₅O₄

There total 7 articles about C₃₂H₃₅Cl₂N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1197342-17-8
3-chloro-1-(2,5-dichlorophenyl)propan-1-one

: 1197342-23-6
C₃₂H₃₅Cl₂N₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrazine hydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere

3.1: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere

4.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide

5.1: sodium perborate / water; tetrahydrofuran

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

With sodium perborate; hydrazine hydrate; potassium phosphate tribasic trihydrate; di-isopropyl azodicarboxylate; potassium acetate; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1197342-18-9
2-(3-bromophenyl)-1-[3-(2,5-dichlorophenyl)-4,5-dihydropyrazol-1-yl]ethanone

: 1197342-23-6
C₃₂H₃₅Cl₂N₅O₄

Guidance literature:: Multi-step reaction with 5 steps

1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere

2: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere

3: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide

4: sodium perborate / water; tetrahydrofuran

5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

With sodium perborate; potassium phosphate tribasic trihydrate; di-isopropyl azodicarboxylate; potassium acetate; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;

Reference yield:

: 106-46-7,84348-21-0
para-dichlorobenzene

: 1197342-23-6
C₃₂H₃₅Cl₂N₅O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / 110 °C

1.2: 20 °C

2.1: hydrazine hydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

2.2: 18 h / 20 °C

3.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere

4.1: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere

5.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide

6.1: sodium perborate / water; tetrahydrofuran

7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

With aluminum (III) chloride; sodium perborate; hydrazine hydrate; potassium phosphate tribasic trihydrate; di-isopropyl azodicarboxylate; potassium acetate; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;