C₂₇H₂₈N₂O₄

Base Information

Chemical Name:C₂₇H₂₈N₂O₄
CAS No.:80249-85-0
Molecular Formula:C₂₇H₂₈N₂O₄
Molecular Weight:444.53
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₈N₂O₄

Chemical Property:

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Technology Process of C₂₇H₂₈N₂O₄

There total 10 articles about C₂₇H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79228-07-2
(2R,12bS)-3-Eth-(E)-ylidene-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine-2-carbaldehyde

: 80249-85-0
C₂₇H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1: BF₃*Et₂O / CH₂Cl₂ / 0 °C

2: i-Bu₂AlH / 1,2-dimethoxy-ethane / -55 °C

3: NaBH₃CN / tetrahydrofuran / from -70 up to room temp.

4: CH₃I, CaCO₃ / H₂O; acetone / Ambient temperature

5: H₂O; tetrahydrofuran

6: CH₂Cl₂; pyridine

7: LiCl / dimethylformamide / 110 °C

8: 64 percent / NaH / dimethylsulfoxide / Ambient temperature

9: 1.) KOH 2.)BF₃ / 1.) EtOH 2.) MeOH

With potassium hydroxide; boron trifluoride diethyl etherate; boron trifluoride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; calcium carbonate; lithium chloride; methyl iodide; In tetrahydrofuran; pyridine; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)90397-1

Reference yield:

: 79235-45-3
(2R,12bS)-2-[1,3]Dithiolan-2-yl-3-eth-(E)-ylidene-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

: 80249-85-0
C₂₇H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: NaBH₃CN / tetrahydrofuran / from -70 up to room temp.

2: CH₃I, CaCO₃ / H₂O; acetone / Ambient temperature

3: H₂O; tetrahydrofuran

4: CH₂Cl₂; pyridine

5: LiCl / dimethylformamide / 110 °C

6: 64 percent / NaH / dimethylsulfoxide / Ambient temperature

7: 1.) KOH 2.)BF₃ / 1.) EtOH 2.) MeOH

With potassium hydroxide; boron trifluoride; sodium hydride; sodium cyanoborohydride; calcium carbonate; lithium chloride; methyl iodide; In tetrahydrofuran; pyridine; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)90397-1

Reference yield:

: 79228-08-3
(2R,12bS)-2-[1,3]Dithiolan-2-yl-3-eth-(E)-ylidene-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one

: 80249-85-0
C₂₇H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1: i-Bu₂AlH / 1,2-dimethoxy-ethane / -55 °C

2: NaBH₃CN / tetrahydrofuran / from -70 up to room temp.

3: CH₃I, CaCO₃ / H₂O; acetone / Ambient temperature

4: H₂O; tetrahydrofuran

5: CH₂Cl₂; pyridine

6: LiCl / dimethylformamide / 110 °C

7: 64 percent / NaH / dimethylsulfoxide / Ambient temperature

8: 1.) KOH 2.)BF₃ / 1.) EtOH 2.) MeOH

With potassium hydroxide; boron trifluoride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; calcium carbonate; lithium chloride; methyl iodide; In tetrahydrofuran; pyridine; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)90397-1