Technology Process of C19H24F4N4O8S
There total 6 articles about C19H24F4N4O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
2: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
palladium on carbon; hydrogen;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere
2: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
3: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
palladium on carbon; hydrogen;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium azide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2: dmap; triethylamine / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere
3: sodium iodide / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere
4: N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere
5: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
6: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
dmap; sodium azide; palladium on carbon; hydrogen; triethylamine; sodium iodide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k