Triphenylmethyl (R,S)-sec-phenethyl ether

Base Information

• Chemical Name: Triphenylmethyl (R,S)-sec-phenethyl ether
• CAS No.: 79481-61-1
• Molecular Formula: C₂₇H₂₄O
• Molecular Weight: 364.487
• Mol file: 79481-61-1.mol

Synonyms:

Chemical Property of Triphenylmethyl (R,S)-sec-phenethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Triphenylmethyl (R,S)-sec-phenethyl ether

There total 3 articles about Triphenylmethyl (R,S)-sec-phenethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

triphenylmethyl alcohol (76-84-6) + 1-Phenylethanol (98-85-1,13323-81-4) → Triphenylmethyl (R,S)-sec-phenethyl ether (39834-50-9,79481-61-1,79481-62-2)

Guidance literature:

With nanoporous MCM-41-SO₃H; In neat (no solvent); at 20 ℃; for 1.25h; Milling;

DOI:10.1016/j.crci.2014.01.003

Reference yield: 89.0%

1-Phenylethanol (98-85-1,13323-81-4) + trityl chloride (76-83-5) → Triphenylmethyl (R,S)-sec-phenethyl ether (39834-50-9,79481-61-1,79481-62-2)

Guidance literature:

With iron(III) chloride; 1-(n-butyl)-3-methylimidazolium triflate; at 40 ℃; for 2.5h; Ionic liquid;

DOI:10.1080/00397910902838888

Reference yield:

benzyl trityl ether (5333-62-0) → Triphenylmethyl (R,S)-sec-phenethyl ether (39834-50-9,79481-61-1,79481-62-2)

Guidance literature:

Multi-step reaction with 2 steps

1: nanoporous MCM-41-SO₃H / acetonitrile / 1.5 h / 20 °C

2: nanoporous MCM-41-SO₃H / neat (no solvent) / 1.25 h / 20 °C / Milling

With nanoporous MCM-41-SO₃H; In acetonitrile;

DOI:10.1016/j.crci.2014.01.003

upstream raw materials:

1-Phenylethanol

trityl chloride

triphenylmethyl alcohol

benzyl trityl ether

Downstream raw materials:

1-Phenylethanol

triphenylmethane

acetophenone