DL-Phenylalanine, 4-bromo-, hydrochloride

Base Information

• Chemical Name: DL-Phenylalanine, 4-bromo-, hydrochloride
• CAS No.: 108540-72-3
• Molecular Formula: C9H10BrNO2.ClH
• Molecular Weight: 280.54600
• Mol file: 108540-72-3.mol

Synonyms:4-bromophenylalanine-hydrochloride;2-amino-3-(4-bromophenyl)propanoic acid hydrochloride;4-Brom-phenylalanin, Hydrochlorid;hydrochloride;2-amino-3-(4-bromophenyl)-propanoic acid hydrochloride;2-Amino-3-(4-bromo-phenyl)-propionic acid;4-bromo-phenylalanine , hydrochloride;

Chemical Property of DL-Phenylalanine, 4-bromo-, hydrochloride

Chemical Property:

• PSA: 63.32000
• LogP: 2.90580

Purity/Quality:

95% ^*data from raw suppliers

2-Amino-3-(4-bromophenyl)propanoicacidhydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DL-Phenylalanine, 4-bromo-, hydrochloride

There total 4 articles about DL-Phenylalanine, 4-bromo-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl 3-(4-bromophenyl)-2-(diphenylmethyleneamino)propanoate (1262785-54-5) → 4-bromophenylalanine-hydrochloride (108540-72-3,122839-59-2,122852-33-9)

Guidance literature:

With hydrogenchloride; In water; Reflux;

Reference yield:

diethyl (acetylamino)<(4-bromophenyl)methyl>propanedioate (71078-92-7) → 4-bromophenylalanine-hydrochloride (108540-72-3,122839-59-2,122852-33-9)

Guidance literature:

With hydrogenchloride; acetic acid; Heating;

Reference yield:

1-bromomethyl-4-bromobenzene (589-15-1) → 4-bromophenylalanine-hydrochloride (108540-72-3,122839-59-2,122852-33-9)

Guidance literature:

Multi-step reaction with 2 steps

2: HCl,CH₃COOH / Heating

With hydrogenchloride; acetic acid;

upstream raw materials:

diethyl (acetylamino)<(4-bromophenyl)methyl>propanedioate

1-bromomethyl-4-bromobenzene

2-acetylaminomalonic acid diethyl ester

t-butyl 3-(4-bromophenyl)-2-(diphenylmethyleneamino)propanoate

Downstream raw materials:

ethyl 2-amino-3-(4-bromophenyl) propanoate

4-bromo-N-(methoxycarbonyl)phenylalanine

N-α-Tosyl-4-bromphenylalanin

2-{4-Methoxy-3-[4-((Z)-2-methoxycarbonyl-vinyl)-phenoxy]-phenyl}-4-oxo-3,4,6,7,9,10,11,12,14,15-decahydro-2H,5H-1,4a,8,13-tetraaza-benzocyclotridecene-8,13-dicarboxylic acid 13-tert-butyl ester 8-(2,2,2-trichloro-ethyl) ester