3-Cyclohexene-1-Methanol Methanesulfonate

Base Information

Chemical Name:3-Cyclohexene-1-Methanol Methanesulfonate
CAS No.:108541-48-6
Molecular Formula:C8H14O3S
Molecular Weight:190.263
Hs Code.:
Mol file:108541-48-6.mol

Synonyms:methyl(tetrahydrobenzyl) sulfonate;tetrahydrobenzyl methanesulfonate;Methanesulfonic acid cyclohex-3-enylmethyl ester;[(Cyclohex-3-en-1-yl)methyl] methanesulfonate;3-cyclohexene-1-methanol methanesulfonate;

Suppliers and Price of 3-Cyclohexene-1-Methanol Methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Cyclohexene-1-methanolMethanesulfonate
250mg
$ 165.00

Medical Isotopes, Inc.
3-Cyclohexene-1-methanolMethanesulfonate
2.5 g
$ 2200.00

Total 4 raw suppliers

Chemical Property of 3-Cyclohexene-1-Methanol Methanesulfonate

Chemical Property:

PSA：51.75000
LogP:2.39970
Storage Temp.:Refrigerator
Solubility.:Dichloromethane, Diethyl Ether, Ethyl Acetate

Purity/Quality:

99% ^*data from raw suppliers

3-Cyclohexene-1-methanolMethanesulfonate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses (3-Cyclohexene-1-Methanol Methanesulfonate) Protected 3-Cyclohexene-1-methanol (C988020). A cyclohexene derivative found in essential oil of various citrus varieties. A reactant used in the preparation Cinitapride (C441990).

Technology Process of 3-Cyclohexene-1-Methanol Methanesulfonate

There total 4 articles about 3-Cyclohexene-1-Methanol Methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 72581-32-9,1679-51-2
cyclohex-3-enylmethanol

: 124-63-0
methanesulfonyl chloride

: 108541-48-6
[(cyclohex-3-en-1-yl)methyl]methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)81240-0

Reference yield: 98.0%

: 103668-33-3,3309-97-5
3-hydroxymethylcyclohexene

: 124-63-0
methanesulfonyl chloride

: 108541-48-6
[(cyclohex-3-en-1-yl)methyl]methanesulfonate

Guidance literature:: In toluene; at 5 - 10 ℃; for 0.5h;

Reference yield:

: 100-50-5,61746-36-9
3-Cyclohexene-1-carboxaldehyde

: 108541-48-6
[(cyclohex-3-en-1-yl)methyl]methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / LiAlH₄

2: Et₃N / CH₂Cl₂

With lithium aluminium tetrahydride; triethylamine; In dichloromethane;
DOI:10.1039/P29860001641