Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester

Base Information

Chemical Name:Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester
CAS No.:121372-64-3
Molecular Formula:C₃₂H₃₄F₆N₂O₂
Molecular Weight:592.625
Hs Code.:

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Chemical Property of Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester

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Technology Process of Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester

There total 4 articles about Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 454-89-7
3-Trifluoromethylbenzaldehyde

: 121372-64-3
Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / H₂O / 1 h / Ambient temperature

2: 48 percent / Mg*Hg, TiCl₄ / 12 h / 0 °C

4: molecular sieves 4A / diethyl ether / 1 h / Ambient temperature

With amalgamated magnesium; 4 A molecular sieve; titanium tetrachloride; In diethyl ether; water;
DOI:10.1021/jo00271a034

Reference yield:

: 121372-62-1
N-{[3-(trifluoromethyl)phenyl]methylidene}methanamine

: 121372-64-3
Benzoic acid 1-[(4R,5R)-1,3-dimethyl-4,5-bis-(3-trifluoromethyl-phenyl)-imidazolidin-2-yl]-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / Mg*Hg, TiCl₄ / 12 h / 0 °C

3: molecular sieves 4A / diethyl ether / 1 h / Ambient temperature

With amalgamated magnesium; 4 A molecular sieve; titanium tetrachloride; In diethyl ether;
DOI:10.1021/jo00271a034