Technology Process of 4-ethoxy-2-(3-hydroxypropyl)-3,6-dimethylphenol
There total 5 articles about 4-ethoxy-2-(3-hydroxypropyl)-3,6-dimethylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-allyl-4-ethoxy-3,6-dimethylphenol;
With
sodium tetrahydroborate; dimethyl sulfate;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
DOI:10.1007/s11172-013-0200-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2 h / 200 °C
2.1: sodium tetrahydroborate; dimethyl sulfate / tetrahydrofuran / 1 h / 20 °C
2.2: 2 h / 20 °C
With
sodium tetrahydroborate; dimethyl sulfate;
In
tetrahydrofuran;
DOI:10.1007/s11172-013-0200-4
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: bromine / chlorobenzene / -10 - 20 °C
2.1: copper(l) iodide; N,N,N,N,-tetramethylethylenediamine / ethanol; N,N-dimethyl-formamide / 5 h / 95 °C
3.1: sodium hydroxide / N,N-dimethyl-formamide / 0.5 h / 50 °C
3.2: 2 h / 60 °C
4.1: 2 h / 200 °C
5.1: sodium tetrahydroborate; dimethyl sulfate / tetrahydrofuran / 1 h / 20 °C
5.2: 2 h / 20 °C
With
sodium tetrahydroborate; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; bromine; dimethyl sulfate; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1007/s11172-013-0200-4
