5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II)

Base Information

• Chemical Name: 5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II)
• CAS No.: 1191416-93-9
• Molecular Formula: C₈₃H₇₃BF₂N₈O₈Zn
• Molecular Weight: 1424.74

Synonyms:

Chemical Property of 5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II)

Chemical Property:

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Safty Information:

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Useful:

Technology Process of 5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II)

There total 1 articles about 5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

H2-5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrin + zinc diacetate (557-34-6) → 5-(4-[2-(4-benzo-[18-crown-6])amido]phenyl)-15-(4-[2-(4-difluoroboron dipyrrinylphenyl)amido]phenyl)-10,20-di(p-tolyl)porphyrinatozinc(II) (1191416-93-9)

Guidance literature:

In methanol; chloroform; satd. soln. of Zn salt in methanol added to soln. of boron complex in CHCl3, refluxed for 2 h; washed (H2O), dried (Na2SO4), purified by column chromy. (silica gel, hexanes:CHCl3 1::90 v/v);

DOI:10.1021/jp9032194

upstream raw materials:

zinc diacetate

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