((C₆H₅)2GeOCHC₆H₅)2

Base Information

Chemical Name:((C₆H₅)2GeOCHC₆H₅)2
CAS No.:83686-76-4
Molecular Formula:C₃₈H₃₂Ge₂O₂
Molecular Weight:665.851
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2GeOCHC<sub>6</sub>H<sub>5</sub>)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((C₆H₅)2GeOCHC₆H₅)2

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Technology Process of ((C₆H₅)2GeOCHC₆H₅)2

There total 1 articles about ((C₆H₅)2GeOCHC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 7366-23-6
diphenylchlorogermane

: 100-52-7
benzaldehyde

: 83686-76-4
((C₆H₅)2GeOCHC₆H₅)2

Guidance literature:: With triethylamine; In tetrahydrofuran; slight excess of Et3N adding dropwise to a mixt. equimolar amts. of Ge deriv. and PhCHO in THF, heating for 1 h at 60°C, filtering and concg.; identified by NMR spectrum;
DOI:10.1016/S0022-328X(00)87639-1

Reference yield:

: 83686-76-4
((C₆H₅)2GeOCHC₆H₅)2

: 83686-78-6
(C₆H₅)2HGeCH(OH)C₆H₅

Guidance literature:: With lithium aluminium tetrahydride; In not given; not isolated, identified by NMR and IR spectra;
DOI:10.1016/S0022-328X(00)87639-1

Reference yield:

: 83686-76-4
((C₆H₅)2GeOCHC₆H₅)2

: 83686-77-5
(C₆H₅)2ClGeCHOHC₆H₅

Guidance literature:: With hydrogenchloride; In hydrogenchloride; Ge deriv. treating with 1 N HCl; identified by NMR spectrum;
DOI:10.1016/S0022-328X(00)87639-1