Technology Process of C29H29BrN2O5
There total 7 articles about C29H29BrN2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) hydroquinone; 2.) NaHCO3, bromine / 1.) water, r.t., 7 d; 2.) water, r.t., 2 h
2: oxalyl chloride / benzene / 4 h / Heating
3: diethyl ether / 17 h
4: 98 percent / silver oxide / dioxane / 3 h / Heating
5: 224 mg / phosphoryl chloride / 2 h / Heating
6: NaBH4 / methanol / 0.08 h
7: 5 mg / pyridine / 5 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; oxalyl dichloride; bromine; sodium hydrogencarbonate; hydroquinone; silver(l) oxide; trichlorophosphate;
In
1,4-dioxane; methanol; diethyl ether; benzene;
DOI:10.1248/cpb.29.76
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 224 mg / phosphoryl chloride / 2 h / Heating
2: NaBH4 / methanol / 0.08 h
3: 5 mg / pyridine / 5 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; trichlorophosphate;
In
methanol;
DOI:10.1248/cpb.29.76
- Guidance literature:
-
Multi-step reaction with 5 steps
1: diethyl ether / 17 h
2: 98 percent / silver oxide / dioxane / 3 h / Heating
3: 224 mg / phosphoryl chloride / 2 h / Heating
4: NaBH4 / methanol / 0.08 h
5: 5 mg / pyridine / 5 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; silver(l) oxide; trichlorophosphate;
In
1,4-dioxane; methanol; diethyl ether;
DOI:10.1248/cpb.29.76
