Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

Base Information

Chemical Name:Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate
CAS No.:115491-86-6
Molecular Formula:C₃₇H₄₃N₃O₁₅S₂*2Na
Molecular Weight:879.871
Hs Code.:

Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

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Suppliers and Price of Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

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Chemical Property of Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

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Technology Process of Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

There total 11 articles about Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65730-02-1
allyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 115491-86-6
Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) t-BuOK / 1.) DMSO 2.) pyridine

2: 84 percent / I₂, DABCO / tetrahydrofuran

3: 54 percent / TsOH / 1,2-dichloro-ethane

4: 1.) NaOH 2.) DCC / 1.) MeOH

5: 1.) H₂SO₄, DCC / 2.) DMF

6: 1.) TEA 2.) NaHCO₃

With 1,4-diaza-bicyclo[2.2.2]octane; sodium hydroxide; TEA; sulfuric acid; potassium tert-butylate; iodine; sodium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(01)81081-9

Reference yield:

: 54400-75-8,64650-83-5,88903-97-3,116347-86-5,140849-88-3,144300-01-6,54400-77-0
allyl 2-acetamido-2-deoxy-β-D-glucopyranoside

: 115491-86-6
Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

Guidance literature:: Multi-step reaction with 9 steps

1: 66 percent / TsOH / dimethylformamide

2: 91 percent / NaOH / dimethylformamide

3: 87 percent / NaBH₃CN, HCl / tetrahydrofuran

4: 1.) t-BuOK / 1.) DMSO 2.) pyridine

5: 84 percent / I₂, DABCO / tetrahydrofuran

6: 54 percent / TsOH / 1,2-dichloro-ethane

7: 1.) NaOH 2.) DCC / 1.) MeOH

8: 1.) H₂SO₄, DCC / 2.) DMF

9: 1.) TEA 2.) NaHCO₃

With 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium hydroxide; TEA; sulfuric acid; potassium tert-butylate; iodine; sodium cyanoborohydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81081-9

Reference yield:

: 63064-48-2,116288-58-5,117299-90-8,126778-02-7,28738-44-5
allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 115491-86-6
Sodium; 2-{[(2S,4S)-4-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-6-benzyloxymethyl-5-sulfooxy-tetrahydro-pyran-2-yloxy)-1-benzyloxycarbonyl-pyrrolidine-2-carbonyl]-amino}-ethanesulfonate

Guidance literature:: Multi-step reaction with 10 steps

1: 98 percent / MeONa

2: 66 percent / TsOH / dimethylformamide

3: 91 percent / NaOH / dimethylformamide

4: 87 percent / NaBH₃CN, HCl / tetrahydrofuran

5: 1.) t-BuOK / 1.) DMSO 2.) pyridine

6: 84 percent / I₂, DABCO / tetrahydrofuran

7: 54 percent / TsOH / 1,2-dichloro-ethane

8: 1.) NaOH 2.) DCC / 1.) MeOH

9: 1.) H₂SO₄, DCC / 2.) DMF

10: 1.) TEA 2.) NaHCO₃

With 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium hydroxide; TEA; sulfuric acid; potassium tert-butylate; iodine; sodium methylate; sodium cyanoborohydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81081-9