C₁₆H₁₁BrO₂

Base Information

• Chemical Name: C₁₆H₁₁BrO₂
• CAS No.: 1423120-24-4
• Molecular Formula: C₁₆H₁₁BrO₂
• Molecular Weight: 315.166
• Mol file: 1423120-24-4.mol

Synonyms:

Chemical Property of C₁₆H₁₁BrO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₁BrO₂

There total 4 articles about C₁₆H₁₁BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylsalicylaldehyde (698-27-1) → C16H11BrO2 (1423120-24-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / acetone / 6 h / Reflux

2: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 6 h / Reflux

With N-Bromosuccinimide; sodium carbonate; dibenzoyl peroxide; In acetone; benzene;

DOI:10.1007/s00044-012-0159-y

Reference yield:

3-methyl-phenol (108-39-4) → C16H11BrO2 (1423120-24-4)

Guidance literature:

Multi-step reaction with 3 steps

1: boric acid / glycerol / 0.17 h / 150 - 160 °C

2: sodium carbonate / acetone / 6 h / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 6 h / Reflux

With N-Bromosuccinimide; boric acid; sodium carbonate; dibenzoyl peroxide; In acetone; glycerol; benzene; 1: |Duff Aldehyde Synthesis;

DOI:10.1007/s00044-012-0159-y

Reference yield:

phenylacetyl chloride (103-80-0) → C16H11BrO2 (1423120-24-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / acetone / 6 h / Reflux

2: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 6 h / Reflux

With N-Bromosuccinimide; sodium carbonate; dibenzoyl peroxide; In acetone; benzene;

DOI:10.1007/s00044-012-0159-y

upstream raw materials:

4-methylsalicylaldehyde

3-methyl-phenol

phenylacetyl chloride

7-methyl-3-phenyl-2H-chromen-2-one

Downstream raw materials:

7-formyl-3-phenylcoumarin

trans-7-(4-methoxystyryl)-3-phenylcoumarin

trans-7-(3,5-dimethoxystyryl)-3-phenylcoumarin