IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

Base Information

Chemical Name:IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI
CAS No.:110981-66-3
Molecular Formula:C₅₂H₄₄FeI₂O₂P₄Pd
Molecular Weight:1240.89
Hs Code.:

IFe(CO)2((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2PdI

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Chemical Property of IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

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Technology Process of IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

There total 2 articles about IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 110981-64-1
FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 67477-87-6
Pd2I2(μ-dpm)2

: 110981-66-3
IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

Guidance literature:: With carbon monoxide; In benzene; Pd- and Fe-complexes were stirred together in benzene with CO bubbling through the soln. for 3 h; filtered, excess of Et2O was added to the filtrate, mixt. was refrigerated (5°C) overnight, in cases when crystals of heterobimetallic complex were contaminated with Pd2-compound (identified by (31)P NMR), mixt. was sepd. manually; elem. anal.;
DOI:10.1039/DT9870002005

Reference yield:

: IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2HPdI⁽¹⁺⁾*BF₄^(1-)=IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2HPdIBF₄

: 110981-66-3
IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

Guidance literature:: In dichloromethane-d2; attempts to isolate cationic complex from the soln. resulted in partialdecompn. to neutral compound; IR evidence;
DOI:10.1039/DT9870002005

Reference yield: 91.0%

: 110981-66-3
IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 111012-29-4
((CH₃)3CNC)(CO)2Fe((C₆H₅)2PCH₂P(C₆H₅)2)2PdI⁽¹⁺⁾*I^(1-)=(((CH₃)3CNC)(CO)2Fe((C₆H₅)2PCH₂P(C₆H₅)2)2PdI)I

Guidance literature:: In dichloromethane; t-BuNC was added to a soln. of FePd-complex in CH2Cl2, mixt. was left for 15 min; soln. was filtered, filtrate concd., Et2O was added, mixt. refrigeratedat 5°C; elem. anal.;
DOI:10.1039/DT9870002005