methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

Base Information

Chemical Name:methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate
CAS No.:1248573-87-6
Molecular Formula:C₃₇H₅₁F₆O₇PSi
Molecular Weight:780.857
Hs Code.:

methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

Synonyms:

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Chemical Property of methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

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Technology Process of methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

There total 1 articles about methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1248573-85-4
methyl (7Z,13E)-2-bis(2,2,2-trifluoroethoxy)phosphoryl-8-methyl-15-[(1,1-dimethylethyl)dimethylsilyloxy]-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

: 64-19-7,77671-22-8
acetic acid

: 1248573-87-6
methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

Guidance literature:: In tetrahydrofuran; water; for 5h; Inert atmosphere;
DOI:10.1021/jo101533h

Reference yield:

: 1248573-87-6
methyl (7Z,13E)-2-[bis(2,2,2-trifluoroethoxy)phosphoryl]-15-hydroxy-8-methyl-6-[(1,1-dimethylethyl)diphenylsilyloxy]pentadeca-7,13-dienoate

: 1248573-56-9
C₃₇H₄₉F₆O₇PSi

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 21 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo101533h