Technology Process of C16H9BrCl2O2
There total 5 articles about C16H9BrCl2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride / 2 h / 120 - 180 °C
2: potassium carbonate / acetone / 12 h / Reflux
3: sodium acetate; acetic acid / 12 h / Reflux
4: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux
With
aluminum (III) chloride; N-Bromosuccinimide; sodium acetate; potassium carbonate; acetic acid; dibenzoyl peroxide;
In
tetrachloromethane; acetone;
1: |Fries Phenol Ester Rearrangement;
DOI:10.1007/s00044-011-9701-6
- Guidance literature:
-
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 12h;
Reflux;
DOI:10.1007/s00044-011-9701-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid / 0.5 h / 20 °C
2: aluminum (III) chloride / 2 h / 120 - 180 °C
3: potassium carbonate / acetone / 12 h / Reflux
4: sodium acetate; acetic acid / 12 h / Reflux
5: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux
With
aluminum (III) chloride; N-Bromosuccinimide; sulfuric acid; sodium acetate; potassium carbonate; acetic acid; dibenzoyl peroxide;
In
tetrachloromethane; acetone;
2: |Fries Phenol Ester Rearrangement;
DOI:10.1007/s00044-011-9701-6
