tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

Base Information

Chemical Name:tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese
CAS No.:97493-99-7
Molecular Formula:C₁₆H₁₁MnO₄
Molecular Weight:322.199
Hs Code.:

Synonyms:

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Chemical Property of tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

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Technology Process of tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

There total 1 articles about tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: methylcyclopentadienyl manganese(I) tricarbonyl

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 97493-99-7
tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

Guidance literature:: With potassium tert-butoxide; HCl; sodium bicarbonate; In N,N-dimethyl-formamide; under Ar or N2; potassium tert-butoxide (40 mmol) was dissolved in anhyd. DMF, followed by Mn-contg. compd. (40 mmol) and Ar-purged ethyl benzoate (50 mmol); stirring for 24 h; HCl was cannulated into the flask; addn. of sodium bicarbonate; soln. was extd. with Et2O; the ether was evapd. with a N2 stream; the solid was dissolved in anhyd. Et2O, the soln. was washed with H2O, dried with MgSO4, filtered, and gradually cooled to -16°C; the compd. was formed overnight; elem. anal.;
DOI:10.1021/om2003656

Reference yield:

: 97493-99-7
tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

: 1345258-01-6
[Mn(CO)2(C₅H₄CH₂COC₆H₅)]

Guidance literature:: In n-heptane; byproducts: CO; Irradiation (UV/VIS); by irradn. of heptane soln.; UV, IR-spectra monitoring;
DOI:10.1021/om2003656

Reference yield:

: 110-86-1
pyridine

: 97493-99-7
tricarbonyl[η5-((2-oxo-2-phenyl)ethyl)cyclopentadienyl]manganese

: 1345258-03-8
[Mn(CO)2(C₅H₅N)(C₅H₄CH₂COC₆H₅)]

Guidance literature:: In n-heptane; byproducts: CO; Irradiation (UV/VIS); by irradn. of heptane soln.; IR-spectra monitoring; Kinetics;
DOI:10.1021/om2003656