ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

Base Information

Chemical Name:ethyl 4-(2,5-dimethoxybenzyl)-3-furoate
CAS No.:887256-17-9
Molecular Formula:C₁₆H₁₈O₅
Molecular Weight:290.316
Hs Code.:

Synonyms:

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Chemical Property of ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

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Technology Process of ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

There total 4 articles about ethyl 4-(2,5-dimethoxybenzyl)-3-furoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86911-85-5
ethyl 4-(2,5-dimethoxyphenyl)-4-hydroxy-2-butynoate

: 887256-17-9
ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / hydroquinone / 1.5 h / 200 °C

2: TMSI / acetonitrile / 0.17 h

With trimethylsilyl iodide; hydroquinone; In acetonitrile;
DOI:10.1016/j.tet.2006.01.096

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 887256-17-9
ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / -78 °C

1.2: hexane; tetrahydrofuran / 0.33 h

1.3: 71 percent / acetic acid / hexane; tetrahydrofuran / 20 °C

2.1: 72 percent / hydroquinone / 1.5 h / 200 °C

3.1: TMSI / acetonitrile / 0.17 h

With n-butyllithium; trimethylsilyl iodide; hydroquinone; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1016/j.tet.2006.01.096

Reference yield:

: 150-78-7
1,4-dimethoxybezene

: 887256-17-9
ethyl 4-(2,5-dimethoxybenzyl)-3-furoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / titanium tetrachloride / CH₂Cl₂ / 0 °C

2.1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / -78 °C

2.2: hexane; tetrahydrofuran / 0.33 h

2.3: 71 percent / acetic acid / hexane; tetrahydrofuran / 20 °C

3.1: 72 percent / hydroquinone / 1.5 h / 200 °C

4.1: TMSI / acetonitrile / 0.17 h

With n-butyllithium; trimethylsilyl iodide; titanium tetrachloride; hydroquinone; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2006.01.096