rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

Base Information

Chemical Name:rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide
CAS No.:1339232-37-9
Molecular Formula:C₂₅H₂₆F₁₇NO₄S
Molecular Weight:759.525
Hs Code.:

Synonyms:

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Chemical Property of rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

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Technology Process of rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

There total 5 articles about rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1336938-40-9
C₁₃H₁₉NO₂

: 1339232-37-9
rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

2: 1 h / 150 °C / Inert atmosphere; Microwave irradiation; Sealed vial

3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

4: dichloromethane / 0.33 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In methanol; dichloromethane; 3: Swern oxidation;
DOI:10.1039/c1cc13992d

Reference yield:

: 1019633-62-5
n-butyl-(3,5-dimethoxybenzyl)amine

: 1339232-37-9
rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1 h / 150 °C / Inert atmosphere; Microwave irradiation; Sealed vial

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

3: dichloromethane / 0.33 h / 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; 2: Swern oxidation;
DOI:10.1039/c1cc13992d

Reference yield:

: 1339232-34-6
n-butyl-(3,5-dimethoxybenzyl)-2-hydroxyacetamide

: 1339232-37-9
rac-N-butyl-N-(3,5-dimethoxybenzyl)-2-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)thio)-2-hydroxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

2: dichloromethane / 0.33 h / 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; 1: Swern oxidation;
DOI:10.1039/c1cc13992d