H₂L⁴

Base Information

Chemical Name:H₂L⁴
CAS No.:1149390-75-9
Molecular Formula:C₃₈H₃₈N₄O₂
Molecular Weight:582.745
Hs Code.:

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Suppliers and Price of H₂L⁴

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of H₂L⁴

Chemical Property:

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Technology Process of H₂L⁴

There total 1 articles about H₂L⁴ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2810-42-6
N,N'-bis(chloroacetyl)-o-phenylenediamine

: 103-49-1
dibenzylamine

: 1149390-75-9
H₂L⁴

Guidance literature:: In ethanol; water; for 24h; Reflux;
DOI:10.1002/ejic.200701122

Reference yield: 48.0%

: 1149390-75-9
H₂L⁴

: 7732-18-5
water

: tetraethylammonium tetrachloroniccolate(II)

: [Ni(C₆H₄(NC(O)CH₂N(CH₂C₆H₅)2)2)]*H₂O

Guidance literature:: With NaH; In N,N-dimethyl-formamide; byproducts: H2; Ni:amine=1:1 molar ratio, a soln. of N compd. treated with NaH (excess),stirred (ca. 15-20 min), a soln. of Ni salt added, stirred for 2 h at r oom temp.; filtered (Celite), concd. (vac.), pptd. (diethyl ether), recrystd. (CH3CN/diethyl ether); elem. anal.;
DOI:10.1002/ejic.200701122