[copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol)

Base Information

• Chemical Name: [copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol)
• CAS No.: 935742-46-4
• Molecular Formula: C₃H₈O*C₁₀H₈N₂*C₁₄H₈O₆S*Cu*H₂O
• Molecular Weight: 602.124
• Mol file: 935742-46-4.mol

Synonyms:

Chemical Property of [copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol)

There total 1 articles about [copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.7%

[2,2]bipyridinyl (366-18-7) + copper(II) chloride hexahydrate + bis(4-carboxyphenyl)sulfone (2449-35-6) + water (7732-18-5) + isopropyl alcohol (67-63-0,8013-70-5) → [copper(II)(4,4'-dicarboxybiphenyl sulfone(-2H))(2,2'-bipyridine)(water)]n*n(isopropanol) (935742-46-4)

Guidance literature:

With aq. NaOH; aq. HCl; In water; N,N-dimethyl-formamide; isopropyl alcohol; High Pressure; mixt. of CuCl2*6H2O, organic ligand, bipyridine, aq. NaOH, aq. HCl, distilled water, isopropanol and DMF sealed in autoclave; heated at 180°C for 72 h under autogeneous pressure; cooled slowly to room temp.; filtrated; washed with distilled water and isopropanol; dried in air; elem. anal.;

DOI:10.1016/j.poly.2006.10.007

upstream raw materials:

[2,2]bipyridinyl

bis(4-carboxyphenyl)sulfone

water

isopropyl alcohol