PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽¹⁺⁾*Cl^(1-)=PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2Cl

Base Information

• Chemical Name: PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽¹⁺⁾*Cl^(1-)=PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2Cl
• CAS No.: 335377-44-1
• Molecular Formula: C₃₅H₃₃NP₃Pt*Cl
• Molecular Weight: 791.108

Synonyms:

Chemical Property of PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽¹⁺⁾*Cl^(1-)=PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2Cl

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Technology Process of PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽¹⁺⁾*Cl^(1-)=PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2Cl

There total 2 articles about PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽¹⁺⁾*Cl^(1-)=PtCN(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

potassium cyanide + [chloro(bis[(2-diphenylphosphino)ethyl]phenylphosphine)platinum(II)] chloride (33847-49-3) → PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2(1+)*Cl(1-)=PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2Cl (335377-44-1)

Guidance literature:

In methanol; Pt-complex was added to soln. of KCN in MeOH, kept at 50°C for 10h with stirring; ether was added, filtered off, washed with water, MeOH and ether, dried,recrystd. from benzene-MeOH; elem. anal.;

DOI:10.1016/S0020-1693(00)00329-7

Reference yield:

bis(2-diphenylphosphinoethyl)phenylphosphine (23582-02-7) → PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2(1+)*Cl(1-)=PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2Cl (335377-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: water; dichloromethane

2: methanol

In methanol; dichloromethane; water;

DOI:10.1016/S0020-1693(00)00329-7

Reference yield:

AuCl(S(CH2CH2OH)2) (69462-32-4) + PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2(1+)*Cl(1-)=PtCN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2Cl (335377-44-1) → PtAuCl2CN(C6H5)2PCH2CH2PC6H5CH2CH2P(C6H5)2

Guidance literature:

In methanol; chloroform-d1; Pt-complex in CDCl3 was reacted with Au-complex in MeOH, mixt. was stirred for 12 h, filtered off; monitored by NMR;

DOI:10.1016/S0020-1693(00)00329-7

upstream raw materials:

[chloro(bis[(2-diphenylphosphino)ethyl]phenylphosphine)platinum(II)] chloride

bis(2-diphenylphosphinoethyl)phenylphosphine

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