trans-[(PdCl(PEt₃)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))]

Base Information

• Chemical Name: trans-[(PdCl(PEt₃)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))]
• CAS No.: 1025721-59-8
• Molecular Formula: C₅₀H₈₀Cl₂N₂O₄P₄Pd₂
• Molecular Weight: 1180.84

Synonyms:

Chemical Property of trans-[(PdCl(PEt₃)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))]

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of trans-[(PdCl(PEt₃)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))]

There total 1 articles about trans-[(PdCl(PEt₃)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-dichlorobis(triethylphosphane)palladium(II) (77027-39-5) + ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine (1025721-38-3) → trans-[(PdCl(PEt3)2)2(ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine(-2H))] (1025721-59-8)

Guidance literature:

With CuI; ((CH₃)2CH)2NH; In dichloromethane; byproducts: C6(OCH3)4(NC6H4CC)2; treatment of ortho-C6(MeO)4(NC6H4CCH)2 with cis-Pd(PEt3)2Cl2 (1 equiv.) in the presence of CuI and (i-Pr)2NH in CH2Cl2;

DOI:10.1021/om7010563

upstream raw materials:

cis-dichlorobis(triethylphosphane)palladium(II)

ortho-bis(ethynylbenzene)-N,N'-tetramethoxyquinone diimine

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