cis-dichlorobis(triethylphosphane)palladium(II)

Base Information

Chemical Name:cis-dichlorobis(triethylphosphane)palladium(II)
CAS No.:77027-39-5
Molecular Formula:C₁₂H₃₀Cl₂P₂Pd
Molecular Weight:413.644
Hs Code.:

Synonyms:

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Chemical Property of cis-dichlorobis(triethylphosphane)palladium(II)

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Technology Process of cis-dichlorobis(triethylphosphane)palladium(II)

There total 13 articles about cis-dichlorobis(triethylphosphane)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 74666-77-6
W(O)(CHC(CH₃)3)Cl₂(P(C₂H₅)3)2

: 110-60-1
1,4-diaminobutane

: 28425-04-9,15642-19-0,77027-39-5
dichlorobis(triethylphosphine)palladium(II)

: 79329-28-5
W(O)(CHC(CH₃)3)Cl₂(CH₃)2NCH₂CH₂N(CH₃)2

Guidance literature:: In toluene; byproducts: 1,5-cyclooctadiene; react. of educts for 2 d; solvent removed in vac., residue dissolved in ether, cooled to -30°C, pentane was added to the filtrate, crystd. at -30°C, product recrystd. from ether/pentane, elem. anal.;

Reference yield: 80.0%

: 40927-17-1,41762-42-9
PdCl₂(PhCN)2

: 74666-77-6
W(O)(CHC(CH₃)3)Cl₂(P(C₂H₅)3)2

: 28425-04-9,15642-19-0,77027-39-5
dichlorobis(triethylphosphine)palladium(II)

: Cl₂W(P(C₂H₅)3)(O)CHC(CH₃)3

Guidance literature:: In toluene; toluene soln. of W and Pd compd. (in 2:1 molar ratio) were stirred for 3 h; mixt. was stirred with activated charcoal for 0.5 h, filtered, toluene removed in vac., pentane was added for crystn., recrystd. from toluene/pentane, elem. anal.;

Reference yield:

: dichlorobis(triethyl phosphine)-μ-dichloro dipalladium (II)

: 28425-04-9,15642-19-0,77027-39-5
dichlorobis(triethylphosphine)palladium(II)

Guidance literature:: With NaBH₄; (Me₂NCH₂CH₂CH₂Te)2; In methanol; acetone; (N2); preparing of NaTeCH2CH2CH2NMe2 by reduction of ditelluride with sodium borohydride, addn. of suspn. of palladium compd., stirring for 4 h; evapn., extn. (hexane), extn. (acetone), passing through Florisil column, evapn., elem. anal.;
DOI:10.1016/j.ica.2005.09.019