C₃₄H₄₅BrO₃S

Base Information

Chemical Name:C₃₄H₄₅BrO₃S
CAS No.:1393475-09-6
Molecular Formula:C₃₄H₄₅BrO₃S
Molecular Weight:613.699
Hs Code.:

C<sub>34</sub>H<sub>45</sub>BrO<sub>3</sub>S

Synonyms:

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Chemical Property of C₃₄H₄₅BrO₃S

Chemical Property:

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Technology Process of C₃₄H₄₅BrO₃S

There total 7 articles about C₃₄H₄₅BrO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86636-47-7
(2Z,6Z)-8-(benzyloxy)-2,6-dimethyl-1-(tetrahydropyran-2-yloxy)-octa-2,6-diene

: 1393475-09-6
C₃₄H₄₅BrO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium / naphthalene

2.1: methanesulfonic acid; triethylamine / tetrahydrofuran / 1 h / Cooling with ice; Inert atmosphere

2.2: 2 h / Cooling with ice; Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / 1.5 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

5.1: pyridine; phosphorus tribromide / diethyl ether / 3 h / Cooling with ice; Inert atmosphere

With pyridine; n-butyllithium; methanesulfonic acid; phosphorus tribromide; lithium; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; naphthalene; diethyl ether; hexane;
DOI:10.1021/ja306184m

Reference yield:

: C₁₅H₂₅BrO₂

: 1393475-09-6
C₃₄H₄₅BrO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / 1.5 h / -78 °C / Inert atmosphere

1.2: 6 h / -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

3.1: pyridine; phosphorus tribromide / diethyl ether / 3 h / Cooling with ice; Inert atmosphere

With pyridine; n-butyllithium; phosphorus tribromide; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane;
DOI:10.1021/ja306184m

Reference yield:

: 52188-74-6,70238-38-9,94854-66-7,115425-27-9,130487-40-0,86636-48-8
(2Z,6Z)-8-(benzyloxy)-2,6-dimethylocta-2,6-dien-1-ol

: 1393475-09-6
C₃₄H₄₅BrO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanesulfonic acid; triethylamine / tetrahydrofuran / 1 h / Cooling with ice; Inert atmosphere

1.2: 2 h / Cooling with ice; Inert atmosphere

2.1: N,N-dimethyl-formamide; acetonitrile / 6 h / 20 °C / Cooling with ice; Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / 1.5 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

5.1: pyridine; phosphorus tribromide / diethyl ether / 3 h / Cooling with ice; Inert atmosphere

With pyridine; n-butyllithium; methanesulfonic acid; phosphorus tribromide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja306184m