4-hydroxy-4-methyl-5-oxohex-1-en-3-yl dimethyl phosphate

Base Information

• Chemical Name: 4-hydroxy-4-methyl-5-oxohex-1-en-3-yl dimethyl phosphate
• CAS No.: 15353-08-9
• Molecular Formula: C₉H₁₇O₆P
• Molecular Weight: 252.204
• Mol file: 15353-08-9.mol

Synonyms:5-Hexen-2-one,3,4-dihydroxy-3-methyl-, 4-(dimethyl phosphate); NSC 102235

Chemical Property of 4-hydroxy-4-methyl-5-oxohex-1-en-3-yl dimethyl phosphate

Chemical Property:

• Vapor Pressure: 1.89E-06mmHg at 25°C
• Boiling Point: 354.6°C at 760 mmHg
• Flash Point: 168.3°C
• Density: 1.198g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-hydroxy-4-methyl-5-oxohex-1-en-3-yl dimethyl phosphate

There total 2 articles about 4-hydroxy-4-methyl-5-oxohex-1-en-3-yl dimethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4r-acetyl-2,2,2-trimethoxy-4-methyl-5c-vinyl-2λ5-[1,3,2]dioxaphospholane → phosphoric acid 1-(1-hydroxy-1-methyl-2-oxo-propyl)-allyl ester dimethyl ester (15353-08-9)

Guidance literature:

With water; In chloroform;

DOI:10.1021/jo01267a055

Reference yield:

2,2,2-trimethoxy-4,5-dimethyl-2,2-dihydro-1,3,2-dioxaphosphole (1665-79-8) → phosphoric acid 1-(1-hydroxy-1-methyl-2-oxo-propyl)-allyl ester dimethyl ester (15353-08-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: H₂O / CHCl₃

With water; In dichloromethane; chloroform;

DOI:10.1021/jo01267a055

upstream raw materials:

2,2,2-trimethoxy-4,5-dimethyl-2,2-dihydro-1,3,2-dioxaphosphole

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