[UCl₄(triphenylphosphine oxide)2]

Base Information

Chemical Name:[UCl₄(triphenylphosphine oxide)2]
CAS No.:58001-79-9
Molecular Formula:C₃₆H₃₀Cl₄O₂P₂U
Molecular Weight:936.421
Hs Code.:

[UCl<sub>4</sub>(triphenylphosphine oxide)2]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [UCl₄(triphenylphosphine oxide)2]

Chemical Property:

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Technology Process of [UCl₄(triphenylphosphine oxide)2]

There total 4 articles about [UCl₄(triphenylphosphine oxide)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 10026-10-5
uranium(IV) chloride

: 791-28-6
Triphenylphosphine oxide

: 58001-79-9,85281-21-6,16923-61-8
[UCl₄(triphenylphosphine oxide)2]

Guidance literature:: In tetrahydrofuran; Glovebox;
DOI:10.1002/anie.201609838

Reference yield: 90.0%

: [UO₂Cl₂(Ph₃PO)2]

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 58001-79-9,85281-21-6,16923-61-8
[UCl₄(triphenylphosphine oxide)2]

Guidance literature:: [UO₂Cl₂(Ph₃PO)2]; With [(trimethylsilyl)methyl]sodium; In tetrahydrofuran; at -108 ℃; for 0.00833333h; Schlenk technique; Inert atmosphere;

dimethylsilicon dichloride; In tetrahydrofuran; for 4h; Reagent/catalyst; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201609838

Reference yield: 85.0%

: 10026-04-7,53609-55-5
tetrachlorosilane

: [UO₂Cl₂(Ph₃PO)2]

: 58001-79-9,85281-21-6,16923-61-8
[UCl₄(triphenylphosphine oxide)2]

Guidance literature:: [UO₂Cl₂(Ph₃PO)2]; With [(trimethylsilyl)methyl]sodium; In tetrahydrofuran; at -108 ℃; for 0.00833333h; Schlenk technique; Inert atmosphere;

tetrachlorosilane; In tetrahydrofuran; for 6h; Reagent/catalyst; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201609838