Technology Process of C40H52N6O4S2
There total 12 articles about C40H52N6O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / methanol; tetrahydrofuran; water / 2 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 2 h / 0 - 20 °C
3: trifluoroacetic acid / chloroform / 8 h / 20 °C
4: potassium carbonate / acetone / 24 h / Reflux
5: tin(II) chloride dihdyrate / methanol / 6 h / Reflux
With
tin(II) chloride dihdyrate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; chloroform; water; acetone;
DOI:10.1039/c2md20219k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 2 h / 0 - 20 °C
2: trifluoroacetic acid / chloroform / 8 h / 20 °C
3: potassium carbonate / acetone / 24 h / Reflux
4: tin(II) chloride dihdyrate / methanol / 6 h / Reflux
With
tin(II) chloride dihdyrate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; chloroform; acetone;
DOI:10.1039/c2md20219k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / chloroform / 8 h / 20 °C
2: potassium carbonate / acetone / 24 h / Reflux
3: tin(II) chloride dihdyrate / methanol / 6 h / Reflux
With
tin(II) chloride dihdyrate; potassium carbonate; trifluoroacetic acid;
In
methanol; chloroform; acetone;
DOI:10.1039/c2md20219k