1-Methyl-1H-pyrrolo[3,2-C]pyridine

Base Information

• Chemical Name: 1-Methyl-1H-pyrrolo[3,2-C]pyridine
• CAS No.: 24331-97-3
• Molecular Formula: C₈H₈N₂
• Molecular Weight: 132.165
• DSSTox Substance ID: DTXSID80559369
• Wikidata: Q82442064

Synonyms:1-METHYL-1H-PYRROLO[3,2-C]PYRIDINE;24331-97-3;N-methyl-5-azaindole;1-METHYLPYRROLO[3,2-C]PYRIDINE;1H-Pyrrolo[3,2-c]pyridine, 1-methyl-;SCHEMBL256341;DTXSID80559369;WIZGGYPJNCGAKV-UHFFFAOYSA-N;1-methylpyrrolo[3, 2-c]pyridine;ZAA33197;MFCD12923814;AKOS027374550;AS-61734;D70942;EN300-748839;Z1255373921

Chemical Property of 1-Methyl-1H-pyrrolo[3,2-C]pyridine

Chemical Property:

• XLogP3: 0.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 132.068748264
• Heavy Atom Count: 10
• Complexity: 124

Purity/Quality:

99% ^*data from raw suppliers

1-Methyl-1H-pyrrolo[3,2-c]pyridine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CN1C=CC2=C1C=CN=C2

Technology Process of 1-Methyl-1H-pyrrolo[3,2-C]pyridine

There total 4 articles about 1-Methyl-1H-pyrrolo[3,2-C]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

5-azaindole (271-34-1) + dimethyl sulfate (77-78-1) → 1-methyl-1H-pyrrolo<3,2-c>pyridine (24331-97-3)

Guidance literature:

5-azaindole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.166667h; Inert atmosphere;

dimethyl sulfate; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol900150u

Reference yield: 66.0%

1-methyl-4-chloro-1H-pyrrolo<3,2-c>pyridine (27382-01-0) → 1-methyl-1H-pyrrolo<3,2-c>pyridine (24331-97-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 5h; under 2280 Torr;

Reference yield: 60.0%

5-azaindole (271-34-1) + methyl iodide (74-88-4) → 1-methyl-1H-pyrrolo<3,2-c>pyridine (24331-97-3)

Guidance literature:

5-azaindole; With Tris(3,6-dioxaheptyl)amine; potassium tert-butylate; In toluene; at 0 - 20 ℃; for 4h;

methyl iodide; In toluene; at 0 - 20 ℃; for 16h;

DOI:10.24820/ARK.5550190.P011.640

upstream raw materials:

1-methyl-4-chloro-1H-pyrrolo<3,2-c>pyridine

5-azaindole

dimethyl sulfate

methyl iodide

Downstream raw materials:

3-formyl-1-methyl-1H-pyrrolo<3,2-c>pyridine

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