C₂₄H₂₉N₁₁O₄

Base Information

Chemical Name:C₂₄H₂₉N₁₁O₄
CAS No.:1461658-54-7
Molecular Formula:C₂₄H₂₉N₁₁O₄
Molecular Weight:535.566
Hs Code.:

C<sub>24</sub>H<sub>29</sub>N<sub>11</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₄H₂₉N₁₁O₄

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Technology Process of C₂₄H₂₉N₁₁O₄

There total 12 articles about C₂₄H₂₉N₁₁O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1461658-48-9
C₁₁H₁₂N₄O₃

: 1461658-53-6
C₁₃H₁₉N₇O₂*C₂HF₃O₂

: 1461658-54-7
C₂₄H₂₉N₁₁O₄

Guidance literature:: C₁₁H₁₂N₄O₃; With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 2h; Inert atmosphere;

C₁₃H₁₉N₇O₂*C₂HF₃O₂; With triethylamine; In dichloromethane; N,N-dimethyl-formamide; for 96h; Inert atmosphere;
DOI:10.1039/c3cc45342a

Reference yield:

: C₁₂H₁₄BrNO₃

: 1461658-54-7
C₂₄H₂₉N₁₁O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2.1: potassium hydroxide / methanol / 16 h / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 2 h / Inert atmosphere

3.2: 96 h / Inert atmosphere

With dmap; sodium azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc45342a

Reference yield:

: 5027-65-6
pyridine-3,5-dicarboxylic acid monomethyl ester

: 1461658-54-7
C₂₄H₂₉N₁₁O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 40 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

4.1: potassium hydroxide / methanol / 16 h / Inert atmosphere

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 40 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

7.1: dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 2 h / Inert atmosphere

8.2: 96 h / Inert atmosphere

With dmap; sodium azide; oxalyl dichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc45342a