1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

Base Information

Chemical Name:1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate
CAS No.:1309151-14-1
Molecular Formula:CF₃O₃S*C₂₃H₃₄NS₂
Molecular Weight:537.732
Hs Code.:

Synonyms:

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Chemical Property of 1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

There total 3 articles about 1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-89-4
piperidine

: 1309151-14-1
1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: acetone / 0.5 h / 0 °C / Inert atmosphere

2: acetonitrile / 2 h / 80 °C / Inert atmosphere

3: tetrafluoroboric acid / water; acetic anhydride / 0.33 h / 20 °C / Inert atmosphere

4: potassium hexamethylsilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

5: benzene / 0.08 h / Inert atmosphere

With tetrafluoroboric acid; potassium hexamethylsilazane; In tetrahydrofuran; water; acetic anhydride; acetone; acetonitrile; benzene;
DOI:10.1002/anie.201100420

Reference yield:

: 1309151-28-7
2-oxo-2-(2,4,6-triisopropylphenyl)ethyl piperidine-1-carbodithioate

: 1309151-14-1
1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrafluoroboric acid / water; acetic anhydride / 0.33 h / 20 °C / Inert atmosphere

2: potassium hexamethylsilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3: benzene / 0.08 h / Inert atmosphere

With tetrafluoroboric acid; potassium hexamethylsilazane; In tetrahydrofuran; water; acetic anhydride; benzene;
DOI:10.1002/anie.201100420

Reference yield:

: 98-77-1
piperidinium piperidyldithiocarbamate

: 1309151-14-1
1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 2 h / 80 °C / Inert atmosphere

2: tetrafluoroboric acid / water; acetic anhydride / 0.33 h / 20 °C / Inert atmosphere

3: potassium hexamethylsilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

4: benzene / 0.08 h / Inert atmosphere

With tetrafluoroboric acid; potassium hexamethylsilazane; In tetrahydrofuran; water; acetic anhydride; acetonitrile; benzene;
DOI:10.1002/anie.201100420