C₁₄H₁₈O₄

Base Information

Chemical Name:C₁₄H₁₈O₄
CAS No.:1327311-89-6
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

C<sub>14</sub>H<sub>18</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₈O₄

Chemical Property:

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Technology Process of C₁₄H₁₈O₄

There total 7 articles about C₁₄H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955030-25-8
C₁₄H₁₈O₃

: 1327311-89-6
C₁₄H₁₈O₄

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.06.087

Reference yield:

: 955030-40-7
C₁₄H₂₀O₃

: 1327311-89-6
C₁₄H₁₈O₄

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / 1 h / -78 °C

2: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 0 - 20 °C

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In water; tert-butyl alcohol; 1: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.087

Reference yield:

: C₁₂H₂₆O₂Si

: 1327311-89-6
C₁₄H₁₈O₄

Guidance literature:: Multi-step reaction with 7 steps

1: titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -20 °C

2: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h

3: ethanol; zinc / 3 h / 80 °C

4: sodium hydride / tetrahydrofuran / 14 h / 0 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / 1 h / -78 °C

7: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 0 - 20 °C

With 1H-imidazole; titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; ethanol; Cumene hydroperoxide; tetrabutyl ammonium fluoride; iodine; sodium hydride; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 1: Sharpless asymmetric epoxidation / 6: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.087