[Fe(α-benzyl dioxymate)2(pyridine)2]

Base Information

• Chemical Name: [Fe(α-benzyl dioxymate)2(pyridine)2]
• CAS No.: 21292-57-9
• Molecular Formula: C₃₈H₃₂FeN₆O₄
• Molecular Weight: 692.557
• Mol file: 21292-57-9.mol

Synonyms:

Chemical Property of [Fe(α-benzyl dioxymate)2(pyridine)2]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Fe(α-benzyl dioxymate)2(pyridine)2]

There total 1 articles about [Fe(α-benzyl dioxymate)2(pyridine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

pyridine (110-86-1) + iron(II) chloride tetrahydrate + benzildioxime (23873-81-6) → [Fe(α-benzyl dioxymate)2(pyridine)2] (21292-57-9,25862-82-2)

Guidance literature:

With sodium acetate trihydrate; In pyridine; methanol; dissolving of FeCl2*4H2O in MeOH and α-benzyldioxime in pyridine and NaCH3COO*3H2O in MeOH, alternate addn. in small portions of soln. sodium acetate and benzyldioxime to soln. of iron chloride with continuous stirring; crystn. for 2 months; elem. anal.;

DOI:10.1134/S0036023610070090

Reference yield:

[Fe(α-benzyl dioxymate)2(pyridine)2] (21292-57-9,25862-82-2) + (((CH3)2C6H2OCH2)2NCH2CH2N(CH3)2)Al(CH3) (925208-50-0) → ((((CH3)2C6H2OCH2)2NCH2CH2N(CH3)2)Al(C6H5CNO)2)2Fe(NC5H5)2

Guidance literature:

In tetrahydrofuran;

DOI:10.1039/c2dt30285c

upstream raw materials:

pyridine

benzildioxime