2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde

Base Information

• Chemical Name: 2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde
• CAS No.: 122347-08-4
• Molecular Formula: C₃₀H₄₆O₃Si
• Molecular Weight: 482.779

Synonyms:

Chemical Property of 2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde

There total 1 articles about 2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(1R,3R,4R,4aR)-1-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-4,7-dimethyl-1,3,4,4a,5,6-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane (120410-11-9) → 2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde (122347-08-4,122407-55-0) + {(3S,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane (120410-18-6) + {(3R,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane (120410-12-0)

Guidance literature:

In toluene; at 190 ℃; for 24h; Yield given. Yields of byproduct given; heating in a sealed tube;

Reference yield: 97.0%

2-{(1R,3R)-3-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-3-methyl-2-[1-trimethylsilanyloxy-meth-(Z)-ylidene]-cyclopentyl}-propionaldehyde (122347-08-4,122407-55-0) + {(3S,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane (120410-18-6) + {(3R,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane (120410-12-0) → (3R,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-ol (122407-52-7) + (3S,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-ol (122440-51-1)

Guidance literature:

With water; pyridinium p-toluenesulfonate; In tetrahydrofuran; water; for 15h; Ambient temperature;

upstream raw materials:

{(1R,3R,4R,4aR)-1-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-4,7-dimethyl-1,3,4,4a,5,6-hexahydro-cyclopenta[c]pyran-3-yloxy}-trimethyl-silane

Downstream raw materials:

(3R,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-ol

(3S,4R,4aR,7S)-7-[(S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-cyclopent-1-enylmethyl]-4,7-dimethyl-3,4,4a,5,6,7-hexahydro-cyclopenta[c]pyran-3-ol

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